IntroductionCIPAC Methods, when proposed by a company or an organization get a first status (draft Method) when they are discussed in a CIPAC Meeting. After having been accepted, they receive the status "provisional" in a following CIPAC Meeting, and finally they are accepted as full methods.
Decisions of the 52th CIPAC Meeting Braunschweig Germany
The table "Decisions of the 52th CIPAC Meeting" presented below the methods which are either accepted as provisional or full methods.
List of decisions Version after 52th CIPAC Meeting Braunschweig
CIPAC No / name
Description
Status
Published 454 alpha-cypermethrin
The soap washing method for the determination of remaining active ingredient concentration remains a tentative MT method because of the ongoing general work on LN washing method(s)
The method extension to the determination of alpha-cypermethrin in LN formulations (CIPAC/4568) with a modified sample preparation for bednets with alpha-cypermethrin incorporated) has been accepted as full CIPAC method subject to modifications in the preparation of the calibration solutions.tentative
full
LN-method, download click here
571 Azoxystrobin
The capillary GC method (CIPAC/4557) for determination of azoxystrobin in TC, WG and SC formulations was accepted as full CIPAC method.
full
prepublished method 761 d,d-trans-Cyphenothrin
The scope of the capillary GC method (CIPAC/4431) for determination of d,d-trans cyphenothrin in TC and EC formulations was changed to cyphenothrin. The method has been accepted as full CIPAC method, subject to the finalisation of the rewording of the method (incl. the submission of the respective chromatograms).
full
no 420 Cyromazine
The reversed phase HPLC method (CIPAC/4559) for the determination of cyromazine in TC, SP and SL formulations was accepted as full CIPAC method.
full
prepublished method 333 Deltamethrin
The extension of the scope of CIPAC method 333 (CIPAC/4497) for the determination of the total content of deltamethrin in LN formulations remains a provisional CIPAC method until further information is received to finalize the editorial process of the method.
The method for the determination of wash retention of LN formulations remains a provisional washing MT method because of the ongoing general work on LN washing method(s).provisional
provisional
LN-method, download click here 484.202 Fenoxaprop-P-ethyl
The method extension (CIPAC/4552) of the reversed phase HPLC method (CIPAC Handbook J, p. 51) for the determination of the chemical purity of fenoxaprop-ethyl to EC and OD formulations was accepted as full CIPAC method.
The method extension (CIPAC/4553) of the enantioselective HPLC method as quantitative identity test for the determination of fenoxaprop-P-ethyl (CIPAC Handbook J, p. 51) in OD formulations was accepted as full CIPAC method.full
full
704 Lufenuron
The reversed phase HPLC method (CIPAC/4561) for the determination of lufenuron in TC and EC formulations was accepted as full CIPAC method.
full
prepublished method 331 Permethrin
he "washing method" (CIPAC/4503) remains as tentative MT method because of the ongoing general work on LN washing method(s).
tentative LN-method, download click here
33 Piperonyl butoxide
The method extension to the capillary GC method (AOAC-CIPAC 32+33+345/TK(M)) for the determination of piperonyl butoxide in TK and AL formulations to EW formulations (CIPAC/4554) was accepted as full CIPAC method.
full
prepublished method 407 Prochloraz
The reversed phase HPLC method (CIPAC/4565) for the determination of prochloraz in TC and EC formulations was accepted as full CIPAC method.
The method for the determination of prochloraz in prochloraz-Zn-complex remains as provisional, subject to further clarifications.
full
provisional
prepublished method 631 Thiacloprid
The reversed phase HPLC method (CIPAC/4550) for the determination of thiacloprid in TC, SC, SE, WG and OD formulations was accepted as full CIPAC method.
full
prepublished method 673 Boscalid
The reversed phase HPLC method (CIPAC/4611) for the determination of boscalid in TC, WG, SC and SE formulations was accepted as provisional CIPAC method, providing the IR spectra for the identity test are submitted
provisional
no 738 Clothianidin
The reversed phase HPLC method (CIPAC/4604) for the determination of clothianidin in TC and WG formulations was recommended for a full scale trial.
no
511 Cyprodinil
The reversed phase HPLC method (CIPAC/4625) for the determination of cyprodinil in TC, EC and WG formulations was accepted as provisional CIPAC method, subject to the clarification for the use of TFA and the introduction of a note concerning the use of the Teflon filter.
provisional
no 35 Fenitrothion
The normal phase HPLC method (CIPAC/4602) for the determination of fenitrothion in TC, WP, EC and UL formulations was accepted as provisional CIPAC method. It was agreed to remove the results of laboratory 5 from the statistical evaluation.
provisional
no 581 Fipronil
The method extension to the reversed phase HPLC method (581/TC, CIPAC Handbook J) for the determination of fipronil in FS, SC, WG, GR and FG formulations (CIPAC/4630) was accepted as provisional CIPAC method subject to introduction of a note concerning the addition of water to avoid insufficient dissolution.
provisional
no 612 Indoxacarb
The chiral normal phase HPLC method (CIPAC/4613) for the determination of indoxacarb in TC, TK, SC, WG and EC formulations was accepted as provisional CIPAC method, subject to substitute n-hexane with n-heptane and to provide chromatograms with heptane.
provisional
no 526.201 Haloxyfop-P-methyl
The chiral normal phase HPLC method (CIPAC/4618) for the determination of haloxyfop-P-methyl in TC and EC formulations was accepted as provisional CIPAC method, subject to clarification regarding the filters of the column and the use of a pressure that is outside of the recommended limits of the column.
provisional
no 651.229 Mefenpyr-diethyl
The reversed phase HPLC method (CIPAC/4627/A) for the determination of mefenpyr-diethyl in TC, and the normal phase HPLC method (CIPAC/4627/B) for the determination of mefenpyr-diethy in WG, OD, EW and EC formulations was accepted as provisional CIPAC method, subject to correction of the calculation in the method description.
provisional
no
MT 194 Adhesion to Treated Seed
The MT method for the determination of adhesion of seed treatment formulations to treated seeds (CIPAC/4580) remains as provisional CIPAC MT method until further clarification. (not published in CIPAC M)
provisional
prepublished method
357 N-nitroso-pendimethalin in pendimethalin The independent laboratory validated HPLC-UV method for the determination of the relevant impurity N-nitroso-pendimethalin in pendimethalin TC as well as in EC formulations was noticed and regarded to be suitable for the determination of the relevant impurity N-nitroso-pendimethalin in pendimethalin TC and EC, subject to clarification of certain points. no
Prepublished CIPAC Methods
There are always some methods which have been accepted as CIPAC Methods, but await publication. Please refer to the page "prepublished Methods" where you find a list of methods which are not yet published in a Handbook, but can be obtained as "prepublished Method" through the CIPAC distribution channel.
last update 29.09.2008