| Title |
| Preface |
| Acknowledgements |
| Contents |
| |
|
Miscellaneous
Techniques |
| Introduction |
|
Freezing point |
MT
1 |
|
Melting point |
MT
2 |
|
Specific gravity and density, |
MT
3.1 hydrometer method |
|
Specific gravity and density, |
MT
3.2 pyknometer method |
|
Specific gravity and density, |
MT
3.3 density of suspension concentrates |
|
Acetone soluble material |
MT
5.2 solution at room temperature |
|
Solubility in acetone |
MT
5 |
|
Acetone soluble material |
MT
5.1 hot solution |
|
Solubility in hexane |
MT
6 |
|
Solubility in ethanol |
MT
7 |
|
Ethanol soluble material, |
MT 7.1 hot solution |
|
Ethanol soluble material, |
MT
7.2 solution at room temperature |
|
Kerosene insoluble material |
MT 8 |
|
Water soluble material |
MT
9 |
|
Water insoluble material, |
MT
10.1 hot solution of the sample |
|
Water insoluble material, |
MT
10.2 cold solution of the sample |
|
Water insoluble material, |
MT
10.3 coarse material-water insoluble |
|
Water insoluble material, |
MT
10.4 insoluble material in pesticide aqueous solutions |
|
Xylene insoluble material |
MT
11 |
| Flash
point, |
MT 12.1 Abel method |
| Flash
point, |
MT
12.2 Tag closed tester |
| Flash
point, |
MT
12.3 Pensky-Martens closed tester |
| Freezing
mixtures, |
MT
14.1 ( 5 ± 1°C) |
| Freezing
mixtures, |
MT
14.2 ( 10 ± 1°C) |
| Suspensibility
of water dispersible powders, |
MT 15.1 CIPAC method |
| Suspensibility
of water dispersible powders, |
MT
15.2 AID method |
| Dichlorodifluoro-methane
|
MT
16 insoluble material |
| Loss
on drying, |
MT
17.1 oven drying at 60°C |
|
Loss on drying, |
MT
17.2 vacuum drying at 45°C, 24 h |
| Loss
on drying, |
MT
17.3 over drying at 100°C at constant weight |
|
Loss on drying, |
MT
17.4 vacuum drying at room temperature |
|
Standard waters, |
MT
18.1 CIPAC standard waters A - G |
|
Standard waters, |
MT
18.2 H and J |
|
Standard waters, |
MT
18.3 non-CIPAC standard waters |
|
Buffer Solutions |
MT
19 Phosphate buffer |
| Phosphate
buffer solutions |
MT
19 |
| Dilute
emulsion stability |
MT 20 |
|
Silica for chromatography, |
MT
21.1 silica |
|
Silica for chromatography, |
MT
21.2 Sorbisil M 60 |
|
Silica for chromatography, |
MT
21.3 Florisil |
| Viscosity,
|
MT
22.1 viscosity of transparent and opaque liquids |
|
viscosity Redwood |
MT
22.2 |
| viscosity
of mineral oil |
MT
22.3 |
| Miscibility
with hydrocarbon oil |
MT 23 |
| Phosphorus
pentoxide desiccant |
MT 24 |
| Sand
for germination tests |
MT 25 |
| John
Innes Potting compost for soil testing of seed germination |
MT 26 |
| Acetone |
MT 27
insoluble material |
| Dimedone
derivative |
MT 28
|
| Sulphated
ash, |
MT 29
general method |
|
Water, |
MT 30
Karl Fischer method |
| Water, |
MT 30.2
Dean and Stark method |
| Water, |
MT 30.3
free water 'speedy' method |
|
Water |
MT 30.4
water in acetone solutions |
|
Free
acidity or alkalinity, |
MT
31.1 methyl red indicator method |
| Free
acidity or alkalinity, |
MT 31.2
electrometric prodedure |
| Free
acidity or alkalinity, |
MT 31.3
acidity of petroleum products |
| Conductivity |
MT 32
determination of |
| Tap density,
|
MT 33
of powders |
| Dustability
test after accelerated storage |
MT 34 |
| Oil insoluble
material |
MT 35 |
| Emulsion
characteristics of emulsifiable concentrates, |
MT 36.1
five per cent v/v oil phase when diluted |
| Emulsion
characteristics of emulsifiable concentrates, |
MT 36.2
dispersion stability of aqueous emulsions |
| Isolation
of active ing redient, |
MT 37.1
extraction with acetone |
|
MT 37.2
extraction with light petroleum |
| Organic
chlorine, |
MT 38.1
potassium-xylene method |
| Organic
chlorine, |
MT 38.2
Stepanov method |
| Organic
chlorine, |
MT 38.3
semi-micro determination of total chlorine |
| Low temperature
stability, |
MT 39.1
emulsifiable concentrates and solutions |
|
Low temperature stability, |
MT
39.2 aqueous solutions |
|
Water content and suspended solids, |
MT 40.1
water content |
|
Water content and suspended solids, |
MT
40.2 suspended solids |
| Dilution
stability |
MT 41
|
| Particle
size, |
MT 42.1
formulations without carriers |
| Particle
size, |
MT 42.2
formulations containing carriers |
| Particle
size distribution of a DDT dispersible powder |
MT 43 |
| Flowability,
|
MT 44
of powders |
| Removal
of dyes |
MT 45 |
| Accelerated
storage tests by heating, |
MT 46.1
general methods |
| Accelerated
storage tests by heating, |
MT 46.2
special methods |
| Foaming,
persistent |
MT 47.1 |
| Foaming,
persistent |
MT 47.2
of suspension concentrates |
| Persistent
foaming |
MT 47.1 |
| Stability
of undiluted tar oil products, |
MT 48.1
miscible type |
| stock
emulsion type |
MT 48.2
|
| Stability
of diluted tar and petroleum oil products, |
MT 49.1
tar-oils-miscible and stock emulsion types |
| Stability
of diluted tar and petroleum oil products, |
MT 49.2
petroleum oil-miscible type |
|
Alumina, |
MT 50
Brockmann activity grade III |
| Stability
of tar-petroleum and petroleum oil products-undiluted, |
MT 51.1
miscible type |
| Stability
of diluted and petroleum oil concentrate products, |
MT 52.1
miscible type |
| Wettability
|
MT 53 |
| Evaluation
of wettability, |
MT 53.1
wetting time of a standard type |
| Evaluation
of wettability, |
MT 53.2
wetting of leaf surfaces |
| Evaluation
of wettability, |
MT 53.3
wetting of dispersible powders |
| Stability
of undiluted DNOC-petroleum, |
MT 54
petroleum and tar-petroleum oil products |
| Stability
of diluted oil products, |
MT 55.1
tar-petroleum oil |
| Stability
of diluted oil products, |
MT 55.2
petroleum and DNOC petroleum oils |
| Stability
of diluted oil products, |
MT 55.3
petroleum oils for orchard use |
| Stability
of diluted oil products, |
MT 55.4
petroleum oils for glasshouse use |
| Volatility
of neutral oil, |
MT 56.1
preliminary examination |
| Volatility
of neutral oil, |
MT 56.2
full method |
| Unsulphonated
residue of neutral oil |
MT 57 |
| Dust
content and apparent density of granular formulations, |
MT 58.1
sampling |
| Dust
content and apparent density of granular formulations, |
MT 58.2
preparation of the sample |
| Dust
content and apparent density of granular formulations, |
MT 58.3
apparent density after compactation without pressure |
| Sieve
analysis, |
MT 59.1
dry sieving-dusts |
| Sieve
analysis, |
MT 59.2
dry sieving-granular products |
| Sieve
analysis, |
MT 59.
3 wet sieving |
| Sieve
analysis, |
MT 59.4
sieve test for granular material |
|
Rate of solution of the sodium salts of phenoxyalkanoic acid
herbicides and their solid formulations |
MT 60 |
| Neutral
oil, |
MT 64
determination of distillation range |
| Hydrolysable
organic chlorine, |
MT 64.1
HCH and lindane, dried residues, or technical materials |
| Hydrolysable
organic chlorine, |
MT 64.2
HCH or lindane dusts and dispersible powders |
| Hydrolysable
organic chlorine, |
MT 64.4
DDT residues of technical material |
| Hydrolysable
organic chlorine, |
MT 64.3
HCH or lindane emulsifiable concentrates and solutions |
| Hydrolysable
organic chlorine, |
MT 64.5
DDT dusts and dispersible powders |
| Hydrolysable
organic chlorine, |
MT 64.6
DDT emulsifiable concentrates and solutions |
| Determination
of organochlorine pesticides in aqueous emulsions |
MT 65 |
| Organochlorine
pesticides, |
MT 65
determination in aqueous emulsions |
| Free
acidity of phenoxyalkanoic esters |
MT 66 |
| Fat extraction
apparatus |
MT 67
|
| Chlorides,
|
MT 68.1
in phenoxyalkanoic acids |
| Free
phenols in phenoxyalkanoic herbicides, |
MT 69
GLC method |
|
Solubility in sodium hydroxide, |
MT 71.1
phenoxy-alkanoic herbicides |
| Solubility
in sodium hydroxide, |
MT 71.2
cresols |
| Solubility
in sodium hydroxide, |
MT 71.3
bromoxynil and ioxynil |
| Hardness
of water |
MT 73
|
| Neutrality
|
MT 74 |
| pH, |
MT 75
determination of |
| Determination
of pH values, |
MT 75.1
general method |
| pH of
aqueous dispersions |
MT 75.2 |
| 1-Chloro-2,3-epoxyethane
|
MT 77 |
| Epichlorhydrin
|
MT 77 |
| Solubility
in triethanolamine |
MT 76 |
| Hydrogen
sulphide and thiols |
MT 78 |
| Acid
wash test |
MT 79 |
|
Residue on evaporation, |
MT 80.1
low boiling products |
| Residue
on evaporation, |
MT 80.2
cresols |
| Soluble
alkalinity |
MT 81 |
| Soluble
chlorides |
MT 82 |
| Seed
adhesion test for powders for seed treatment |
MT 83 |
| Ignition
tests, assessment of spontaneous ignition potential of dithio-carbamates
|
MT 84.1 |
| Kieselguhr,
for GLC |
MT 86.1 |
| Kieselguhr,
for GLC |
MT 86.2
for partition chromatography |
| Chloroform
solubles |
MT 81.1
hot solutions |
| Chloroform
solubles |
MT 87.2
cold solutions |
|
Toluene solubles |
MT 90 |
| Lead,
|
MT 92.1
dithizone general method |
| Lead,
|
MT 92.2
dithizone method B |
| Manganese,
|
MT 93.1
bismuthate method |
| Manganese,
|
MT 93.2
EDTA method |
| Zinc, |
MT 94.1
in dithiocarbamates |
| Iron,
|
MT 95
determination of |
|
Separation and identification of herbicides |
MT
97 |
| Copper,
water soluble |
MT 98.1
colorimetric method with bathocuproine |
| Copper,
water soluble |
MT 98.2
atomic absorption method |
| Arsenic,
|
MT 99
determination of |
|
Chlorides, |
MT 100
total chlorides |
| Total
chlorides |
MT 100 |
| Heptane-insoluble
material |
MT 101 |
| Nitron
complexes, |
MT 105
preparation of |
Ammonia-ammonium
chloride buffer
solution-pH 10 |
MT 107 |
| Dinitro
compounds, |
MT 108
solubility of salts and alkali insolubles |
| Solubility
of salts and alkali insoluble-dinitro compounds |
MT 108 |
| Dinitro
compounds, |
MT 109
mineral acidity of |
| Mineral
acidity of dinitrocompounds |
MT 109 |
|
Mercury |
MT 110
Mercurial impurities in technical and formulated mercury compounds
|
| Silanization
of gas chromatographic columns |
MT 113 |
| Correction
of interfering peaks |
MT 114 |
| Mercury(II)
salts, |
MT 116
characteristic reactions of |
| Chlorides, |
MT 117
test for |
| Iodides,
|
MT 118
test for |
|
Phosphates, |
MT 120
test for |
| Silicates, |
MT 121
test for |
| Extractable
acids, |
MT 126
determination of |
|
Extractable acids, |
MT
127 melting point of |
| Gas
chromatography of phenoxyalkanoic acids and other herbicides
|
MT 129 |
| Dithiocarbamates,
|
MT 130
Identity test for certain alkylenebis(dithiocarbamates) |
|
Identity test for certain dithiocarbamates and thiram and
their mixtures |
MT 130 |
| Nitrophenols,
|
MT 133
determination of |
| 2-Aminopyridine, |
MT 134
preparation of complexes of nitro compounds |
| Identification
of urea herbicides |
MT 137 |
| Urea
herbicides, |
MT 137
identification of |
| Pour
point of mineral oil |
MT 139 |
|
Free amines in urea herbicides |
MT 141 |
| Detection
and identification of impurities in substituted phenylurea
herbicides |
MT 142 |
|
Phenylurea herbicides, |
MT
142 detection and identification of impurities in substituted
|
|
Phosphorus in active ingredients, |
MT
145 spectrophotometric determination after TLC separation
|
| Oil
content of emulsifiable concentrates |
MT 146 |
| Retention
test of seed treatment powders |
MT 147 |
| Pourability
of suspension concentrates |
MT 148 |
| Packing
of columns for gaschromatography |
MT 149 |
|
TCDD, |
MT 151.1
determination in 2,4,5-T technical |
| TCDD,
|
MT 151.2
in 2,4,5-T technical esters |
| Amines |
MT 152
identification of |
| Identification
of amines |
MT 152 |
| Dithiocarbamates,
|
MT 153
Qualitative procedure for confirmation of the presence of
a dithiocarbamate or thiuram disulphide |
| Qualitative
procedure for confirmation of the presence of dithio-carbamates
or thiuram disulfide |
MT 153 |
|
Thiram, |
MT
153 qualitative procedure for confirmation of the presence
of |
| Dithiocarbamates,
|
MT 154
determination of anions |
| Free
phenols in phenoxyalkanoic herbicides, |
MT 155
HPLC method |
| Water
solubility, |
MT 157.1
preliminary test |
| Water
solubility, |
MT 157.2
column elution method |
| Water
solubility, |
MT 157.3
flask method |
| Mercury,
determination on treated seed |
MT 158 |
| Pour
and tap bulk density of granular materials |
MT 159 |
|
Spontaneity of dispersion, |
of suspension
concentrates MT 160 |
| Suspensibility
of aqueous suspension concentrates |
MT 161 |
| ETU,
|
MT 162
determination in ethylenebisdithiocarbamates |
| Cypermethrin,
|
MT 163
identity test |
| Fenvalerate,
identity test |
MT 163 |
| Identity
tests for permethrin, cypermethrin and fenvalerate |
MT 163 |
|
Permethrin, |
MT
163 identity test |
| Bupirimate, |
MT 164
identity test |
| Ethirimol, |
MT 164
identity test |
| Identity
tests for pirimicarb, bupirimate, ethirimol, pirimiphos-ethyl
and pirimiphos-methyl |
MT 164 |
| Primicarb, |
MT 164
identity test |
| Pirimiphos-ethyl,
|
MT 164
identity test |
| Pirimiphos-methyl,
|
MT 164
identity test |
| Ultraviolet
absorption test for ethylenebisdithiocarbamates |
MT 165 |
| Sampling
of water dispersible granules |
MT 166 |
| Sieve
analysis, |
MT 167
wet sieving-water dispersible granules |
| Suspensibility
of water dispersible granules |
MT 168 |
| Tap
density, |
MT 169
of water dispersible granules |
|
Sieve analysis, |
MT 170
dry sieving-water dispersible granules |
| Dustiness
of granular products |
MT 171 |
| Flowability,
|
MT 172
of water dispersible granules |
| Dilute
emulsion stability |
MT 173
colorimetric method |
| Emulsion
characteristics of emulsifiable concentrates, |
MT 173
dilute, colorimetric determination of the stability of emulsions
|
| Spontaneity
of dispersion, |
MT 174
of water dispersible granules |
| Determination
of seed-to-seed uniformity of distribution for liquid seed-treament
formulations |
MT 175 |
| Seed
treatment formulations, liquid, determination of seed-seed
uniformity of distribution |
MT 175 |
| Dissolution
rate of water-soluble bags |
MT 176 |
| Water
soluble bags, |
MT 176
dissolution rate of |
| Suspensibility
of water dispersible powders, |
MT 177
simplified CIPAC method |
| |
|
Appendix |
| Appendix
A Index of Chemical Code Numbers, Numerical List |
| Appendix
B Index of Chemical Code Numbers, Alphabetical List |
| Appendix
C Codes for Ions and Ester radicals |
| Appendix
D Code for Formulation |
| Appendix
E Membership of CIPAC |
| Appendix
F Index of MT-Methods |
| Cumulative
Index |